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Journal/NDM52 2018 eng — различия между версиями

(Contents of issue 4 (volume 52).)
 
(не показано 18 промежуточных версий этого же участника)
Строка 1: Строка 1:
New Data on Minerals. 2018. Volume 52. <br>
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'''New Data on Minerals, Volume 54, 2020'''<br>
Edited by P.Yu. Plechov, Professor, Doctor in Science. <br>
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__TOC__
Published by the Fersman Mineralogical Museum, Russian Academy of Sciences.<br>
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====='''DEADLINES FOR ARTICLES'''=====
<br>
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Issue 1 - March 31, 2020<br>
Four issues of the journal in 2018:
+
Issue 2 - May 31, 2020<br>
====Contents of issue 1 (volume 52). Revision articles and brief reports on the study of museum samples.====
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Issue 3 - August 31, 2020<br>
{{NDM_article
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Issue 4 - November 30, 2020<br>
| Авторы = Plechov P.Yu. (Editorial)
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=====Editorial Board=====
| Название = Changes in the editorial policy of the journal "New data on minerals", p. 1-2
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'''Editor in Chief:'''<br>
| Файл = Plechov2018-1_rus.pdf
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Plechov P.Yu. - Doctor of Geology and Mineralogy, Professor<br>
| Приложения =
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'''Members of Editorial Board:'''<br>
}}{{NDM_article
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Garanin V.K. - Doctor of Geology and Mineralogy, Professor<br>
| Авторы = Gritsenko Yu.D.  
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Novgorodova M.I. - Doctor of Geology and Mineralogy, Professor<br>
| Название = Titanium garnets collection of the A.E.Fersman Mineralogical Museum of the Russian Academy of Sciences, p. 3-5
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Borutsky B.E. - Doctor of Geology and Mineralogy<br>
| Файл = Gritsenko2018-1_rus.pdf
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Spiridonov B.E. - Doctor of Geology and Mineralogy<br>
| Приложения = Gritsenko2018-1_supp_rus.xlsx
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Kamenetsky V.S. - Professor (University of Tasmania)<br>
}}{{NDM_article
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Nenasheva S.N. - PhD in Geology and Mineralogy<br>
| Авторы = Pautov L.A., Mirakov M.A., Shchodibekov M.A.
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Matvienko E.N. - PhD in Geology and Mineralogy<br>
| Название = The discovery of herzenbergite in the granite miarol pegmatite of Vez-Dar in the South-Western Pamir (Tajikistan), p. 6-14
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Generalov M.E. - PhD in Geology and Mineralogy<br>
| Аннотация =
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Pautov L.A. - Senior Researcher <br>
| Файл = Pautov2018-1_rus.pdf
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'''Layout Designer''' <br>
| Приложения =
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Kronrod E.V. - PhD in Chemistry<br>
}}{{NDM_article
 
| Авторы = Shcherbakov V.D., Plechov P.Yu.
 
| Название = P- bearing olivine from lava flow of 2012-2013 Tolbachik volcano eruption, p. 15-17
 
| Аннотация = 160 high-precision microprobe analyzes of olivine from lava and tephra of volcanic Tolbachik eruption are published in the paper. Hot-state lava and tephra were collected during the eruption. Phosphorus rich zones in olivine were formed during the skeletal growth in lava during flow on the surface.
 
| Файл = Shcherbakov_Plechov2018-1_eng.pdf
 
| Приложения = Sherbakov_Plechov2018-1_supp_eng.xlsx
 
}}{{NDM_article
 
| Авторы = Vlasov E.A., Nikolaev Yu.N., Apletalin A.V., Pustovalov V.Yu.
 
| Название = Copper minerals from metamorphogenic veins of the headwaters of the river Ilirneivaem, Chukotka, p. 18-19
 
| Аннотация =
 
| Файл = Vlasov2018-1_rus.pdf
 
| Приложения =
 
}}{{NDM_article
 
| Авторы = Generalov M.E., Pautov L.A.  
 
| Название = Second Lieutenant Chernik Porpecite, p. 20-24
 
| Аннотация = When studying the samples of papetzite transferred to the collection of the Mineralogical Museum by the G.P. Chernik in 1909, it was found that in addition to the proper pappelite (palladium gold of 600-700 probes), they contain native palladium and sulphide phases of Pd<sub>4</sub>S composition. It was also found out that placers, where platinum minerals were found at the end of the XIX century, are located not in Georgia, as indicated in the literature, but in Turkey, near the city of Artvin.
 
| Файл = Generalov_Pautov2018-1_rus.pdf
 
}}{{NDM_article
 
| Авторы = Generalov M.E.
 
| Название = Faberge and Abraxas, p. 25-29
 
| Аннотация =
 
| Файл = Generalov2018-1_rus.pdf
 
}}{{NDM_article
 
| Авторы = Pekov I.V.  
 
| Название = In memoream of E.I.Semenov (1927-2017), p. 30-32
 
| Аннотация =
 
| Файл = Pekov2018-1_rus.pdf
 
| Приложения =
 
}}
 
  
====Contents of issue 2 (volume 52). Articles and brief reports on the study of mineralogical objects.====
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===Content===
 +
==== ''Issue 1'' ====
 
{{NDM_article
 
{{NDM_article
| Авторы = Pautov L.A., Shchodibekov M.A., Mirakov M.A., Faiziev A.R., Khvorov P.V. 
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| Авторы = Smolyaninova V.N.
| Название = Uranopolycrase (U,Y)(Ti,Nb)<sub>2</sub>O<sub>6</sub> from the miarolic pegmatite Museum in the area of ​​the Kukhilal field (South-Western Pamir, Tajikistan)
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| Название = Devoted to the 100th anniversary of the birth of Natalia Nikolaevna Smolyaninova, pp. 1-18
| Файл = Pautov2018-2_rus.pdf
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| Аннотация = Natalia Nikolaevna Smolyaninova (1919–2013) was a mineralogist, daughter of the famous mineralogist Nikolai Alekseevich Smolyaninov. She worked at IGEM of the Academy of Sciences of the USSR, studied mineralogy of the radium-uranium-vanadium deposit Tyuya-Muyun (Kyrgyzstan) and tungsten-molybdenum deposits Akchatau and Batystau (Kazakhstan). She was editor-in-chief of five of the 12 issues of the encyclopedic guide "Minerals".
| Приложения =
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| Файл =  
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| Приложения =  
 
}}{{NDM_article
 
}}{{NDM_article
| Авторы = Ivanova Yu.A., Vlasov E.A.
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| Авторы = Karpenko V.Yu., Pautov L.A., Shodibekov M., Makhmadsharif S., Mirakov M.A.
| Название = Rutile K-feldspar-quartz veins of headwaters of the river Dvoynaya, Western Chukotka
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| Название = Coconinoite: find at the Zor-Yarchi-Chak ore occurrence, Eastern Pamir, pp. 19-25
| Файл = Ivanova2018-2_rus.pdf
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| Аннотация = The find of coconinoite Fe2Al2 (UO2) 2 (PO4) 4 (SO4) (OH) 2 ∙ 20H2O in the oxidation zone at the uranium occurrence Zor-Yarchi-Chak (right bank of the South Ak-Baital River, Eastern Pamir, Tajikistan) is described. The mineral is found in cracks of essentially quartz rock in the form of dense clay-like masses of yellowish color (up to 2 cm2 in area), consisting of lamellar individuals 5–10 microns in diameter across. The refractive index nm = 1.589 (3) at 589 nm. The IR spectrum of the mineral is given. Composition (molecular weight, wt.%, Average for 24 analyzes; range for Al and Fe; H2O - CNH analysis, average for 2 analyzes, wt.%): Al2O3 6.95 (5.44–7.70), Fe2O3 11.13 ( 9.77–12.91), UO3 39.09, P2O5 18.35, SO3 4.64, H2O 22.7, total 102.86. The overestimation of the amount may be associated with partial dehydration of the mineral during microprobe analysis. The empirical formula is Fe2.07Al2.12U + 62.08P3.93S0.88О24 (OH) 2 · 18.16H2O (calculated on 24O + 2OH). Unit cell parameters: a = 12.45 (1), b = 12.87 (1), c = 22.75 (1), β = 105.66 (4). An analysis of the variations of Al and Fe in coconinoite from different locations (up to the high-aluminum non-iron analogue, Koscheka, Uzbekistan) confirms the existence of a natural series with extreme Al and Fe dominant members.
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| Файл =  
 
| Приложения =
 
| Приложения =
 
}}{{NDM_article
 
}}{{NDM_article
| Авторы = Pavlova T.M.
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| Авторы = Pautov L.A., Karpenko V.Yu., Mirakov M.A., Alinazarov U.S., Shodibekov M.A., Iskandarov F.Sh.
| Название = Academician A.E.Fersman scientific readings. History. Chronology.  
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| Название = About bismuthocolumbite from myarolite granite pegmatites in the Eastern Pamirs, pp. 26-37
| Файл = Pavlova2018-2_rus.pdf
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| Аннотация = Findings of bismuthocolumbumite in myarolite granite pegmatites of the Rangkul pegmatite field in the Eastern Pamirs, Gorno-Badakhshan Autonomous Okrug, Tajikistan are described. The mineral was found in the form of crystals up to 2 cm in the myarol cavities of the pegmatite veins Mika, Malysh and in the form of sprouts of 20–30 μm in Sc-containing columbite-Mn in intergrowth with eschinitis- (Y) in the near-myarol complex of pegmatite Dorozhny. The crystals were measured on a goniometer; the calculated and measured coordinates of the faces are given (in the setup a <c <b). The habitus of the crystals is prismatic, determined by the faces of the rhombic prism m {110}; minor and weakly expressed faces of the prismatic belt: pinacoid {010}, prisms {130}, {150}, {160}, {170}; the usual faces of the head are the rhombic prism i {101} and the dipyramid u {111}, the more rare prism f {032}. The color of bismuthocolumbite in crystals is dark brown, almost black, shines reddish-brown, in small fragments reddish-brown to light brown. The trait is light brown. Cleavage perfect according to (010). The measured density, g / cm3, 7.36 (1) (Kid), 7.61 (1) (Mika). Optically biaxial (+), 2V = 70 (10) °, the dispersion is strong, r> v. The plane of the optical axes is perpendicular to the (010) plane. The refractive indices of bismuth-columbite from Mick's pegmatite: np = 2.42 (1), nm = 2.45 (1), ng = 2.50 (2). In reflected light, gray with a faint bluish tint, medium reflectivity, strong anisotropy, strong reflections from yellow to reddish-brown. Reflection spectra are given. Microhardness VHN100 = 360 (Kid), 353 (Mika). 6 m. analyzes. Chem. composition (wt.%, selective an., Kid, Mika, Dorozhniy): Ta2O5 2.11, 11.66, 8.61; Nb2O5 35.54, 28.11, 8.61; WO3 0.08, 0.11, 3.60; TiO2 0.02, 0.00, 0.58; PbO 0.10, 0.10, 0.00; SnO2 0.03, 0.12, 0.00; MnO 0.00, 0.01, 0.26; FeO 0.03, 0.00, 0.11; Sb2O3 0.78, 1.77, 8.55; Bi2O3 62.50, 57.59, 49.75; amount 101.19, 99.47, 100.10. X-ray powder diffraction patterns are shown. Parameters of the rhombic unit cell (Å): a = 4.982 (2), b = 11.719 (4); c = 5.677 (2) (Kid); a = 4.981 (2), b = 11.746 (4); c = 5.670 (2) (Mika). Possible reasons for the rarity of bismuthocolocolumbite as compared to stibiocolumbite and their Ta analogues are discussed.
| Аннотация = The chronology of the scientific readings of Academician Fersman is given. The authors of the scientific reports and the topics are presented, as well as the time and place of the readings.
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| Файл =
In the article 1 table, list of literature from 5 titles. The article contains 1 table, references (5 titles).
 
 
| Приложения =
 
| Приложения =
 
}}{{NDM_article
 
}}{{NDM_article
| Авторы = Shchipalkina N.V., Kononov O.V., Pekov I.V., Koshlyakova N.N., Britvin S.N.
+
| Авторы = Kasatkin A.V.
| Название = Wollastonite and ferrobustite of the Tyrnyauz ore field (North Caucasus): chemical composition, relations and mineralogical-technological aspect
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| Название = To the question of re-studying mineralogical samples from museum collections. I. General Aspects, pp. 38-51
| Файл = Schipalkina2018-2_rus.pdf
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| Аннотация = The article is devoted to the problem of re-studying the samples of minerals stored in museum collections. Two main areas of revision of museum material are examined in detail. One of them is the re-study of the originals of the first study of minerals (type specimens), specifically aimed at clarifying the essential characteristics of insufficiently studied mineral species. The second direction covers all other samples stored in museum collections. The results of their re-study can be the discovery of new mineral species or clarification of the characteristics of already known minerals, finds, including the first, of rare minerals in a certain region and, in any case, an increase in the degree of knowledge or reliability of the diagnosis of a particular mineral. The significance of the results of such studies determines the relevance of the re-study of museum material and increases the value of museum collections.
| Аннотация = Samples previously identified as wollastonite, "ferrowollastonite", "Mn-wollastonite", parawolastonite, bustamite, and ferrobustite from different parts of the Tyrnyauz ore field (Kabardino-Balkaria, Northern Caucasus, Russia) were studied by electron probe microanalysis, infrared spectroscopy, powder and single-crystal radiography. It was found that two rock-forming minerals are presented at this site: wollastonite Ca<sub>3</sub>Si<sub>3</sub>O<sub>9</sub> and ferrobustite Ca<sub>2</sub>Ca<sub>2</sub>FeCa[Si<sub>3</sub>O<sub>9</sub>]<sub>2</sub>, which are macroscopically indistinguishable from each other and can be found in the same mineral assemblages and capable of forming close intergrowths with each other, in which the boundaries between these minerals are always sharp. Wollastonite and ferrobustite can be easily identified by the method of infrared spectroscopy, and also differ in chemical composition. Thus, the FeO and MnO contents in wollastonite and ferrobustamite of the Tyrnyauz field vary in the following limits (wt.%): 0.0-1.2 and 0.1-1.1 (in total - from 0.1 to 2.3) in wollastonite, 7.4 - 10.2 and 1.3 - 3.7 (in the total - from 10.2 to 12.8) in ferrobustamite. Solid solutions between wollastonite and ferrobustamite were not fixed. The prevalence in the skarns of Tyrnyauz ferrobustamite seems to be a serious problem hampering the exploration and production of wollastonite, and makes it necessary to develop a special technique that makes it possible to distinguish conditioned wollastonite raw materials from mineral associations containing ferrobustite and unfit for practical use.
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| Файл =
 
| Приложения =
 
| Приложения =
}}{{NDM_article
 
| Авторы = Ivanova D.A., Shcherbakov V.D., Plechov P.Yu., Nekrylov N.A., Davydova V.O., Turova M.A., Stepanov O.V.
 
| Название = Cristobalite in extrusive rocks of Bezymianny volcano
 
| Файл = IvanovaD2018-2_eng.pdf
 
| Аннотация = We present the first data on the systematic study of compositional and morphological variability of cristobalite in extrusive rocks of Bezymianny volcano (Kamchatka). Andesites and dacites of all seven studied extrusive domes contain cristobalite, which content reaches up to 6 vol.%, and thus may be considered as rock-forming mineral. We distinguish 4 different morphological types of cristobalite – 1) isometric grains surrounded by pores with the characteristic fish-scale cracking; 2) the “prismatic” cristobalite grains in clusters; 3) “pea”-type grains in the matrix glass; 4) “feathery”-type crystals. There were not revealed any clear dependencies between the morphological type of cristobalite, its composition and the composition of host extrusive rocks. Content of minor elements in cristobalite (mainly Al and Na) is up 10 wt.% on an oxide basis. The main mechanism of their isomorphic substitution is Si4+→Al3++(Na+, K+), which can reflect the existence of a solid solution of cristobalite with isostructural to it carnegieite end-member. The entry of Ti (up to 0.27 wt.% of TiO2), Fe (up to 0.43 wt.% of FeO) and Ca (up to 0.15 wt.% of CaO) into the cristobalite structure is described. Cristobalite from extrusive rocks of Bezymianny volcano has the widest range of composition in comparison with all previously published analyses of this mineral.
 
| Приложения =
 
 
}}
 
}}
====Contents of issue 3 (volume 52).====
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==== ''Issue 2'' ====
 
{{NDM_article
 
{{NDM_article
| Авторы = Kasatkin A.V., Levitskiy V.V., Nestola F.  
+
| Авторы = Kasatkin A.V., Skoda R., Chukanov N.V.  
| Название = Supergene minerals of Malyi Mukulan deposit (Tyrnyauz ore field, Northern Caucasus)
+
| Название = To the question of re-studying mineralogical samples from museum collections. II. Cannonite and legernite from the Bukuk deposit (Transbaikalia), pp. 53-60
| Аннотация = An interesting supergene sulfate-arsenate mineralization was discovered by us at the Malyi Mukulan Sn-Bi deposit, Tyrnyauz ore field, Kabardino-Balkaria, Northern Caucasus. A group of sulfates - bianchite, hexahydrite, gypsum, pickeringite, rozenite, cuprian siderotil, chalcanthite and epsomite, as well as arsenates of erythrite-kottigite series and pharmacosiderite were established and studied by EMPA, SXRD and PXRD.
+
| Аннотация = Rare bismuth sulfates, cannonite Bi2O (SO4) (OH) 2 and legernite Bi12.67O14 (SO4) 5 were established by us as a result of re-study of bismuthine samples from the tungsten deposit Bukuk (Eastern Transbaikalia), stored in the systematic collection of the Fersman Mineralogical Museum of RAS, numbered 56077. Both minerals are closely fused together in polymineral pseudomorphs along coarse bismuth crystals, forming veins up to 4 cm long and up to 0.5 cm thick. Empirical formulas: Cannonite Bi2.06S0.97O5 (OH) 2, Bi12 legernite. 67S5.00O34. The parameters of monoclinic unit cells: for cannonite a = 7.691 (1), b = 13.874 (2), c = 5.6569 (8) Å, β = 109.23 (1) °, V = 569.90 (9) ų and Z = 4; in legernite: a = 11.197 (2), b = 5.714 (1), c = 11.879 (2) Å, β = 99.37 (2) °, V = 749.9 (2) ų and Z = 1. Strong bands in spectra: for cannonite 111, 121, 144, 184, 221, 318, 437, 450, 560, 619, 983, 1059, 3439 cm – 1, for legernite 150, 183, 216, 313, 474, 969 cm – 1. Both minerals were found for the first time in the Russian Federation.
| Файл = Kasatkin2018-3_rus.pdf
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| Файл =  
| Приложения =
 
}}{{NDM_article
 
| Авторы = Gorelikova N.V., Portnov A.M., Taskaev V.I., Rassulov V.A., Chizhova I.A., Karimova O.V., Balashov F.V., Boyeva N.M.
 
| Название = Vanadium dravite from the South-East Uzbekistan
 
| Аннотация = V-bearing magnesian tourmaline relate to dravite from South- East Uzbekistan has been studied. This mineral is acicular, the colour is grassy. It is found out at quartz veins with the width up to 10 cm cutting Protorezoic black siliceous schists. Protorozoic schists have a high relation of К/Rb (800) that is typical for tholeitic basalts of oceanic type with a high content of Ti and V. The schists are also enriched in V and U (up to 50 ppm). V<sub>2</sub>O<sub>3</sub> value in tourmaline varies and come to 3%. The negative correlation between V and Al has been established with methods correlation and R-factor analyses that indicates on the substitution Аl<sup>3+</sup>  by  V<sup>3+</sup> at the structure of tourmaline. The studied V-bearing tourmalines are characterized by a higher magnesiality (dravite variety), a low content of Fe<sup>2+</sup> , Fe<sup>3+</sup>, Ti<sup>4+</sup> and also of Аl<sup>3+</sup>, Са<sup>2+</sup>. Evidently, quartz-tourmaline veins are connected with the Hercinian granitoid magmatism attending numerous Au-Ag deposits of the South East Uzbekistan. Appearance of V in the quality a chromophor in metamorphic rocks is an indicator of old oceanic structures at the continents.  
 
| Файл = Gorelikova2018-3_rus.pdf
 
 
| Приложения =
 
| Приложения =
 
}}
 
}}
====Contents of issue 4 (volume 52).====
 
{{NDM_article
 
| Авторы = Shiryaev A.A., Titkov S.V.
 
| Название = Spatial distribution of “Amber” defects in diamond: results of IR mapping
 
| Аннотация =
 
| Файл = Shiriaev2018-4_eng.pdf
 
| Приложения =
 
}}{{NDM_article
 
| Авторы = Pautov L.A., Mirakov M.A., Shodibekov M.A., Fayziev A.R., Khvorov P.V., Makhmadsharif S.
 
| Название = Occurrence of Tungstenite-2H in magnesian skarns of gem quality spinel deposit Kukhi-Lal (South-Western Pamir, Tajikistan)
 
| Аннотация =
 
| Файл = Pautov2018-4_rus.pdf
 
| Приложения =
 
}}{{NDM_article
 
| Авторы = Karpenko V.Yu., Pautov L.A., Agakhanov A.A., Siidra O.I.
 
| Название = On the cadmium mineralization in the Darai-Pioz alkaline massif
 
| Аннотация = Greenockite, CdS (hex.), and otavite, CdCO<sub>3</sub>, have been found for the first time in the Darai-Pioz alkaline massif (Tadzhikistan). Greenockite (with Zn, ranges 3.3 – 3.8 wt. %) forms grains to 0.4 mm in galena aggregations from an aegirine-quartz-feldspar assemblage, in association with polylithionite, cesium-kupletskite, riebeckite-arfvedsonite series amphibole, turkestanite, and anglesite. Hexagonal cell dimensions are as follows: a = 4.171(2), c = 6.772(1) Å. Otavite occurs on a galena micro-vein contact with granulated quartz, as fine aggregations (~0.5 x 0.5 mm), on which Cd- bearing cerussite has developed (CdO 2.3 wt.%). The chemical  composition of otavite is variable  (mol. %): 77 – 87  CdCO<sub>3</sub>, 4 – 19 CaCO<sub>3</sub>, 4 – 9  PbCO<sub>3</sub>, 1 – 5  ZnCO<sub>3</sub>. Cd, and some trace elements were analysed in sphalerite from this massif; Cd ranges there from  0.12 to 3.65 wt. %.  Minerals were investigated by microprobe with EDS and WDS, X-ray, and optical microscopy. A reflective spectrum is shown for greenockite. Possible methods of Zn and Cd differentiation are discussed. This may be the first identification of these minerals in alkaline massifs.<br>
 
There are 5  tables, 7 drawings, and  56 references in the paper.<br>
 
Keywords: cadmium, greenockite, otavite, cerussite cadmium-bearing, galena, sphalerite cadmium-bearing, Darai-Pioz alkaline massif
 
| Файл = Karpenko2018-4_rus.pdf
 
| Приложения =
 
}}
 
<br>
 
[[Journal/NDM51_2018|Russian version (V. 52)]]
 

Текущая версия на 15:48, 4 июня 2020

New Data on Minerals, Volume 54, 2020

DEADLINES FOR ARTICLES

Issue 1 - March 31, 2020
Issue 2 - May 31, 2020
Issue 3 - August 31, 2020
Issue 4 - November 30, 2020

Editorial Board

Editor in Chief:
Plechov P.Yu. - Doctor of Geology and Mineralogy, Professor
Members of Editorial Board:
Garanin V.K. - Doctor of Geology and Mineralogy, Professor
Novgorodova M.I. - Doctor of Geology and Mineralogy, Professor
Borutsky B.E. - Doctor of Geology and Mineralogy
Spiridonov B.E. - Doctor of Geology and Mineralogy
Kamenetsky V.S. - Professor (University of Tasmania)
Nenasheva S.N. - PhD in Geology and Mineralogy
Matvienko E.N. - PhD in Geology and Mineralogy
Generalov M.E. - PhD in Geology and Mineralogy
Pautov L.A. - Senior Researcher
Layout Designer
Kronrod E.V. - PhD in Chemistry

Content

Issue 1

Smolyaninova V.N. Devoted to the 100th anniversary of the birth of Natalia Nikolaevna Smolyaninova, pp. 1-18

Natalia Nikolaevna Smolyaninova (1919–2013) was a mineralogist, daughter of the famous mineralogist Nikolai Alekseevich Smolyaninov. She worked at IGEM of the Academy of Sciences of the USSR, studied mineralogy of the radium-uranium-vanadium deposit Tyuya-Muyun (Kyrgyzstan) and tungsten-molybdenum deposits Akchatau and Batystau (Kazakhstan). She was editor-in-chief of five of the 12 issues of the encyclopedic guide "Minerals".



Karpenko V.Yu., Pautov L.A., Shodibekov M., Makhmadsharif S., Mirakov M.A. Coconinoite: find at the Zor-Yarchi-Chak ore occurrence, Eastern Pamir, pp. 19-25

The find of coconinoite Fe2Al2 (UO2) 2 (PO4) 4 (SO4) (OH) 2 ∙ 20H2O in the oxidation zone at the uranium occurrence Zor-Yarchi-Chak (right bank of the South Ak-Baital River, Eastern Pamir, Tajikistan) is described. The mineral is found in cracks of essentially quartz rock in the form of dense clay-like masses of yellowish color (up to 2 cm2 in area), consisting of lamellar individuals 5–10 microns in diameter across. The refractive index nm = 1.589 (3) at 589 nm. The IR spectrum of the mineral is given. Composition (molecular weight, wt.%, Average for 24 analyzes; range for Al and Fe; H2O - CNH analysis, average for 2 analyzes, wt.%): Al2O3 6.95 (5.44–7.70), Fe2O3 11.13 ( 9.77–12.91), UO3 39.09, P2O5 18.35, SO3 4.64, H2O 22.7, total 102.86. The overestimation of the amount may be associated with partial dehydration of the mineral during microprobe analysis. The empirical formula is Fe2.07Al2.12U + 62.08P3.93S0.88О24 (OH) 2 · 18.16H2O (calculated on 24O + 2OH). Unit cell parameters: a = 12.45 (1), b = 12.87 (1), c = 22.75 (1), β = 105.66 (4). An analysis of the variations of Al and Fe in coconinoite from different locations (up to the high-aluminum non-iron analogue, Koscheka, Uzbekistan) confirms the existence of a natural series with extreme Al and Fe dominant members.



Pautov L.A., Karpenko V.Yu., Mirakov M.A., Alinazarov U.S., Shodibekov M.A., Iskandarov F.Sh. About bismuthocolumbite from myarolite granite pegmatites in the Eastern Pamirs, pp. 26-37

Findings of bismuthocolumbumite in myarolite granite pegmatites of the Rangkul pegmatite field in the Eastern Pamirs, Gorno-Badakhshan Autonomous Okrug, Tajikistan are described. The mineral was found in the form of crystals up to 2 cm in the myarol cavities of the pegmatite veins Mika, Malysh and in the form of sprouts of 20–30 μm in Sc-containing columbite-Mn in intergrowth with eschinitis- (Y) in the near-myarol complex of pegmatite Dorozhny. The crystals were measured on a goniometer; the calculated and measured coordinates of the faces are given (in the setup a <c <b). The habitus of the crystals is prismatic, determined by the faces of the rhombic prism m {110}; minor and weakly expressed faces of the prismatic belt: pinacoid {010}, prisms {130}, {150}, {160}, {170}; the usual faces of the head are the rhombic prism i {101} and the dipyramid u {111}, the more rare prism f {032}. The color of bismuthocolumbite in crystals is dark brown, almost black, shines reddish-brown, in small fragments reddish-brown to light brown. The trait is light brown. Cleavage perfect according to (010). The measured density, g / cm3, 7.36 (1) (Kid), 7.61 (1) (Mika). Optically biaxial (+), 2V = 70 (10) °, the dispersion is strong, r> v. The plane of the optical axes is perpendicular to the (010) plane. The refractive indices of bismuth-columbite from Mick's pegmatite: np = 2.42 (1), nm = 2.45 (1), ng = 2.50 (2). In reflected light, gray with a faint bluish tint, medium reflectivity, strong anisotropy, strong reflections from yellow to reddish-brown. Reflection spectra are given. Microhardness VHN100 = 360 (Kid), 353 (Mika). 6 m. analyzes. Chem. composition (wt.%, selective an., Kid, Mika, Dorozhniy): Ta2O5 2.11, 11.66, 8.61; Nb2O5 35.54, 28.11, 8.61; WO3 0.08, 0.11, 3.60; TiO2 0.02, 0.00, 0.58; PbO 0.10, 0.10, 0.00; SnO2 0.03, 0.12, 0.00; MnO 0.00, 0.01, 0.26; FeO 0.03, 0.00, 0.11; Sb2O3 0.78, 1.77, 8.55; Bi2O3 62.50, 57.59, 49.75; amount 101.19, 99.47, 100.10. X-ray powder diffraction patterns are shown. Parameters of the rhombic unit cell (Å): a = 4.982 (2), b = 11.719 (4); c = 5.677 (2) (Kid); a = 4.981 (2), b = 11.746 (4); c = 5.670 (2) (Mika). Possible reasons for the rarity of bismuthocolocolumbite as compared to stibiocolumbite and their Ta analogues are discussed.



Kasatkin A.V. To the question of re-studying mineralogical samples from museum collections. I. General Aspects, pp. 38-51

The article is devoted to the problem of re-studying the samples of minerals stored in museum collections. Two main areas of revision of museum material are examined in detail. One of them is the re-study of the originals of the first study of minerals (type specimens), specifically aimed at clarifying the essential characteristics of insufficiently studied mineral species. The second direction covers all other samples stored in museum collections. The results of their re-study can be the discovery of new mineral species or clarification of the characteristics of already known minerals, finds, including the first, of rare minerals in a certain region and, in any case, an increase in the degree of knowledge or reliability of the diagnosis of a particular mineral. The significance of the results of such studies determines the relevance of the re-study of museum material and increases the value of museum collections.



Issue 2

Kasatkin A.V., Skoda R., Chukanov N.V. To the question of re-studying mineralogical samples from museum collections. II. Cannonite and legernite from the Bukuk deposit (Transbaikalia), pp. 53-60

Rare bismuth sulfates, cannonite Bi2O (SO4) (OH) 2 and legernite Bi12.67O14 (SO4) 5 were established by us as a result of re-study of bismuthine samples from the tungsten deposit Bukuk (Eastern Transbaikalia), stored in the systematic collection of the Fersman Mineralogical Museum of RAS, numbered 56077. Both minerals are closely fused together in polymineral pseudomorphs along coarse bismuth crystals, forming veins up to 4 cm long and up to 0.5 cm thick. Empirical formulas: Cannonite Bi2.06S0.97O5 (OH) 2, Bi12 legernite. 67S5.00O34. The parameters of monoclinic unit cells: for cannonite a = 7.691 (1), b = 13.874 (2), c = 5.6569 (8) Å, β = 109.23 (1) °, V = 569.90 (9) ų and Z = 4; in legernite: a = 11.197 (2), b = 5.714 (1), c = 11.879 (2) Å, β = 99.37 (2) °, V = 749.9 (2) ų and Z = 1. Strong bands in spectra: for cannonite 111, 121, 144, 184, 221, 318, 437, 450, 560, 619, 983, 1059, 3439 cm – 1, for legernite 150, 183, 216, 313, 474, 969 cm – 1. Both minerals were found for the first time in the Russian Federation.